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tests |
results |
specifications |
1. appearance
2. solubilities
3. identification test a test b test c
test d
test e
5. color of solution (5% solution)
6. ph of solution ( 10 % solution)
7.ortho compound
8. residue insoluble in anhydrous ethanol
9. assay (%)
|
white crystalline powder
conforms
conforms conforms conforms
conforms
conforms
conforms
9.2
conforms
conforms
99.9
|
white to slight yellow crystalline powder
freely soluble in water insoluble in benzene, chloroform & ether.
solution a turns red litmus paper r blue & then bleached it. melting point: 137-140c ignite 1g (cautiously, because of the risk of deflagration). dissolve the residue in 10ml of water r. the solution gives reaction (a) of chlorides.
the solution prepared for identification test c gives reaction (a) of sulfates. the solution prepared for identification test c gives reaction (b) of sodium.
nmt 50 apha
8.0 to 10.0
melting point nlt 134°c
max. 2.0%
nlt 98.0 % nmt 103.0% |